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Article
Publication date: 1 March 2013

Costas A. Charitidis and Dimitrios A. Dragatogiannis

The purpose of this paper is to investigate the use of nanoindentation with a Berkovich indenter as a method of extracting equivalent stress‐strain curves for the base metal and…

Abstract

Purpose

The purpose of this paper is to investigate the use of nanoindentation with a Berkovich indenter as a method of extracting equivalent stress‐strain curves for the base metal and the welded zone of a friction stir welded aluminum alloy.

Design/methodology/approach

Friction stir welding is a solid‐state joining process, which emerged as an alternative technique to be used in high strength alloys that were difficult to join with conventional joining techniques. This technique has a significant effect on the local microstructure and residual stresses combined with deformation. Nano‐ and micro‐indentation are the most commonly used techniques to obtain local mechanical properties of engineering materials. In order to test the reliability of nanoindentation technique and to connect nanoscale with macroscale, the indentation hardness‐depth relation established by Nix and Gao was applied on the experimental values.

Findings

The predictions of this model were found to be in good agreement with classical hardness measurements on AA 6082‐T6 aluminum alloy. Also, finite element method provides a numerical tool to calculate complex nanoindentation problems and in correlation with gradients theories forms a well‐seried tool in order to take into account size effects.

Originality/value

By studying this alloy, the paper reviews fundamental principles such as stress‐strain distribution, size effects rise during nanoindentation and the applicability of finite element method, in order to take into account these issues.

Details

International Journal of Structural Integrity, vol. 4 no. 1
Type: Research Article
ISSN: 1757-9864

Keywords

Article
Publication date: 1 March 2013

Costas A. Charitidis, Dimitrios A. Dragatogiannis and Elias P. Koumoulos

Lightweight alloys are of major concern, due to their applicability, in transport and industry applications. The purpose of this paper is to perform a comprehensive analysis of…

1785

Abstract

Purpose

Lightweight alloys are of major concern, due to their applicability, in transport and industry applications. The purpose of this paper is to perform a comprehensive analysis of time dependent properties of aluminum alloy by nanoindentation technique, through investigation of creep behavior. Additionally, possible explanations on the time dependent behavior and the influence of the hold period at maximum load and the loading rate on the elastic modulus and hardness results are also analyzed and discussed.

Design/methodology/approach

In this work, a comprehensive analysis of time dependent properties of aluminum alloy by nanoindentation technique was performed, by varying the loading rate, the maximum applied load and the loading time. The stress exponent values are derived from the displacement‐holding time curves. The present experimental setup includes three different approaches: variation of loading rate, maximum applied load and loading time. The creep deformation mechanisms of the alloy, which are dependent on experiment setup, are discussed and the characteristic “elbow” behavior in the unloading part of the curves is also reported.

Findings

The authors found that the stress exponent values obtained are dependent on the applied peak loads and indentation loading rates. Nanoindentation creep testing of aluminum AA6082‐T6 revealed significant creep displacements, where the strain rate reached a steady state after a certain time and the stress decreased with time as the displacement increased during the creep process. The slopes of strain rate versus stress curves (exponent of power‐law creep) for different maximum loads and various holding times, were investigated.

Originality/value

The stress exponent of the constant‐load indentation creep, in all three types of experiments, was found to reduce at low load region. In case of different holding load and time, the stress exponent increased almost linearly and increased very rapidly as the indent size increased, exhibiting an intense size effect.

Details

International Journal of Structural Integrity, vol. 4 no. 1
Type: Research Article
ISSN: 1757-9864

Keywords

Article
Publication date: 1 February 2016

Dimitrios A. Dragatogiannis, Elias P. Koumoulos, Ioannis A Kartsonakis and Costas A. Charitidis

The study of nanoindentation as a reliable method to extract creep properties as well as for fundamental understanding of deformation mechanisms at small length scales is an open…

Abstract

Purpose

The study of nanoindentation as a reliable method to extract creep properties as well as for fundamental understanding of deformation mechanisms at small length scales is an open interesting field. The observed creep behavior is attributed to time-dependent plastic deformation based on loading rates. There is a lot of work in the field of nanoindentation in order to understand the dynamic effects on nanomechanical properties. The paper aims to discuss these issues.

Design/methodology/approach

The deformation mechanism is investigated under two experimental approaches (high and low loading rates, respectively) during nanoindentation. The effect of loading rate in the nanomechanical properties, during nanoindentation creep of zinc layer on hot dip galvanized (HDG) steel, is discussed through nanoindentation.

Findings

Analysis of this research effort is emphasized on nanoindentation stress exponent, a critical parameter for the life time and reliability of nano/micro-materials and systems. The corrosion resistance was studied by electrochemical impedance spectroscopy (EIS) and localized EIS.

Originality/value

The study of nanoindentation as a reliable method to extract creep properties as well as for fundamental understanding of deformation mechanisms at small length scales is an open interesting field. The observed creep behavior is attributed to time-dependent plastic deformation based on loading rates. The deformation mechanism is investigated under two experimental approaches (high and low loading rates, respectively) during nanoindentation. The effect of loading rate in the nanomechanical properties, during nanoindentation creep of zinc layer on HDGsteel, is discussed through nanoindentation. Analysis of this research effort is emphasized on nanoindentation stress exponent, a critical parameter for the life time and reliability of nano/micro- materials and systems. The corrosion resistance was studied by EIS and localized EIS.

Details

International Journal of Structural Integrity, vol. 7 no. 1
Type: Research Article
ISSN: 1757-9864

Keywords

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